Reprinted from: R. Rollefson and H. Richards, "Laboratory Experiments in Elementary Physics," Waveland Press, Inc. (Copied by permission.)
PURPOSE OF LABORATORY
In developing a grasp of physics, the beginning student can draw on a variety of resources: textbooks, lectures and demonstrations, problem solving, discussion sessions, and the laboratory.
The laboratory furnishes a unique opportunity for testing physical principles in a quantitative fashion against the actual behavior of nature. Laboratory experience provides the student a more realistic feeling for the origin and limitations of physical concepts; it teaches him to be aware of experimental errors, of ways to minimize them and how to estimate the reliability of the result of an experiment; it introduces him to the need for keeping clear and accurate records of experimental investigations.
RECORD KEEPING
The first requirement of good laboratory work is a good
notebook. We recommend a large bound or spiral notebook
with paper of good enough quality to stand occasional
erasures (needed most commonly in improving pencil sketches
or graphs . . . correction of numbers should always be done
by crossing them out, thus
,
because occasionally one finds later that the original
number was right; the correction a mistake). Coarse (1/4")
cross-ruled pages are more versatile than blank or lined
pages, being useful for tables, crude graphs, and sketches,
while still providing the horizontal lines needed for plain
writing. Put everything that you commit to paper right
into your notebook. Avoid any scribbling of notes on loose
pages; such scraps are always getting lost. A good plan is
to write initially only on the right-hand pages, leaving
the left page for afterthoughts you may decide to put in
later, and also for the kind of exploratory calculations
that you would be tempted to do on scratch paper.
Heading of Experiment. Copy from manual number and name of experiment. Write down date of experiment and name of partner.
Original data in notebook. Original data must always go directly into your notebook, as they are gathered. By "original data" is meant the actual readings you have taken. For example, suppose you know your micrometer caliper is in error by .006 mm. You should record the actual readings taken on the caliper, and then correct the average. In this way, it will be clear that you have made the corrections. Also, when you take 5 or 6 successive readings of a measurement, record each reading, not just the average. From the scatter of the readings, the reader can get an estimate of the precision of the measurement. When both partners record data, errors of recording can be discovered. Record serial numbers of equipment, if given, so that you can find the same equipment if you have to check results later. The data should be arranged in tabular form when appropriate and each item or table should be properly labeled.
Housekeeping deletions. You may think that a notebook combining all work would soon become quite a mess, with a proliferation of erroneous and superseded material. Indeed it might, but you can improve matters greatly with a little housekeeping work every hour or so. Jut draw a box around any erroneous or unnecessary material and hatch three or four parallel diagonal lines across this box. (This way you can come back and rescue the deleted calculations later if you should discover that the first idea was right after all. It occasionally happens.)
Append a note to the margin of the box explaining to yourself what was wrong.
You are expected to keep your notes up, from minute to minute, as you go along. You are not encouraged to take a lot of time at home to "write it up"-you probably have more important things to do than merely making a beautiful notebook.
Remarks and sketches. "Pictorial" sketches of apparatus are normally not recommended. On the other had, a simple diagrammatic sketch is often the simplest and clearest way to define the various quantities indicated in a table of data: a phrase or sentence introducing each table or calculation is essential for making sense out of the notebook record. When a useful result occurs at any stage, describe it with at least a word or phrase. At the end of an experiment, you need some sort of written comment usually including a brief summary table of results.
Graphs. Create graphs directly upon the cross-
hatched paper of your notebook. Show points as circles or
crosses, i.e.,
, or X. Instead of
connecting points by straight lines, draw a smooth curve
which may actually miss most of the points but which shows
the functional relationship between the plotted quantities.
Original data in graphic form (such as the equipotential
contours of the potentials and fields lab) you should also
fasten directly into your book.
Units; coordinate labels. Physical quantities always require a number and a unit to have meaning. Likewise, graphs have abscissas and ordinates which always need labeling.
Data and results. A neat summary of data and results will make your notebook more meaningful to both you and your instructor.
PARTNERS
Limitations of space and equipment usually require that one works with a partner. In addition, it is often stimulating to discuss your work with someone as you go along.
Independent calculations; checks. If possible both partners should perform completely independent calculations. Mistakes in calculation are inevitable, and the more complete the independence of the two calculations, the more complete is the check against these mistakes. Poor results on experiments are often the result of computational errors.
COMPLETION OF WORK
Your instructor will check your work before you leave the lab, and may write down some comments, suggestions, or questions at the end of your work.
Your instructor can help deepen your understanding and "feel" for the subject. Take advantage of opportunities to talk over your work with him.
ERRORS
The value of measurements is greatly enhanced by accompanying them with an estimate of their reliability. Thus, saying that the average diameter of a cylinder is 10.00 + 0.02 mm tells much more than the statement that the cylinder is a centimeter in diameter.
The term "error" is used in physics interchangeable with uncertainty. "Error" in physics does not have the same meaning as mistake. Mistakes, such as errors in calculations, should be corrected before estimating the experimental error. In estimating the reliability of a single quantity such as the diameter of a cylinder, sources of error of a number of different kinds must be taken into account. Firstly there may be an actual variation of the quantity being measured, i.e., the diameter of the cylinder may actually be different in different places. One must then specify where the measurement was made, or, if he wants the diameter in order to calculate the volume, he must find the average diameter by means of a number of measurements at carefully selected places, and the scatter of the measurements will give a first estimate of the reliability of the average diameter.
Secondly, the micrometer caliper with which the measurement is made may be in error. The errors introduced in this way will of course not be distributed equally on both sides of the true value so that averaging a large number does no good. They may be eliminated (or at least reduced) by calibrating the measuring instrument: in the case of the micrometer caliper by taking the zero error (the reading when the jaws are closed) and the readings on selected precision gauges, of dimensions approximately equal to those of the cylinder to be measured. Errors of this type are called systematic.
There is another type of systematic error which occurs in the measurement of a cylinder. The micrometer will always measure the largest diameter between its jaws, so that if there are small bumps or depressions on the cylinder, the average of a large number of measurements will not give the true average diameter but a quantity somewhat larger. (This error can of course be reduced by making the jaws of the caliper smaller in cross section.)
Finally, if one is measuring something of definite size with a calibrated instrument, there are still errors of measurement which, one hopes, are as often positive as negative and will therefore average out, if a large number of trials is taken. For example, the reading of the micrometer caliper may vary because it is not closed with the same force every time, and because the observer's estimate of the fraction of the smallest division varies from trial to trial. It is clear that the average of a number of these measurements should be closer to the true value than any one measurement, and the deviations of the individual measurements from the average give an indication of the reliability of that average value.
Average Deviation
If one finds the average of the absolute values of the deviations, this "average deviation from the mean" is often taken as a measure of reliability. For example, let column 1 represent 10 readings of the diameter of a cylinder taken at one place so that variations in the cylinder do not come into consideration.
Measurements | Deviation from Ave. |
9.943 mm | .000 |
9.942 | .001 |
9.944 | .001 |
9.941 | .002 |
9.943 | .000 |
9.943 | .000 |
9.945 | .002 |
9.943 | .000 |
9.941 | .002 |
9.942 | .001 |
Ave = 9.943 | Ave = .0009 |
Diameter = 9.943 + .001mm |
Expressed algebraically, the average deviation from the mean
is
_m = |x_i - x|n
where is the ith measurement of n taken and
is the mean or arithmetic average of the
readings.
Standard Deviation
A more useful measure of the spread in a set of
measurements is the standard deviation s (or root mean
square deviation). One defines s as
s = [ _i=1^n (x_i - x)^2n
]^12 ,
where is the mean or arithmetical average of the
set of n measurements and
is the ith measurement.
The standard deviation s clearly weighs large deviations more heavily than the average deviation thus giving a less optimistic estimate of the reliability. Careful analysis shows that even a better estimator (and appreciably less optimistic for small sets of measurements) is n/(n-1)s = [ _i=1^n (x_i - x)^2n - 1 ]^12 ,
This estimator is the ``universe" or ``parent" standard deviation and its square,
, the
variance. (For an explanation of the
factor see e.g. Parratt, "Probability and Experimental
Errors in Science," Wiley and Sons, 1961, p. 89f.)
If the errors are distributed about the true value in what
is called a "normal" manner (i.e. the errors have a
gaussian distribution, , about zero), then on
average 68% of a large number of measurements will lie
closer than
to the true value.
Relative error and percentage error
Let be the error in a measurement whose value
is a. Then
is called the relative error of
the measurement, and 100
is the percentage
error. These terms are useful in laboratory work.
Errors in measurements with several independent quantities
If the desired result is the sum or difference of two
measurements, the absolute uncertainties can be added. Let
x and y be the errors in and
respectively. For the sum we have
and the
relative error is
. Since
the signs of
and
can be opposite,
adding the absolute values gives a pessimistic estimate of
the uncertainty. It can be shown that if errors have a
normal or Gaussian distribution and are independent, they
should be added by taking the square root of the sum of the
squares, i.e.,
z = x^2 + y^2.
For the difference of two measurements we obtain a relative
error of
which can of
course become very large if x is nearly equal to y. This
result shows that it is wise to avoid, if possible,
designing an experiment where one measures two large
quantities and takes their difference to obtain the desired
quantity.
If the result wanted is a power of the quantity measured,
one computes the uncertainty of the result as follows. Let
a be the measurement, the error and
the result desired. Then
z = (a ±)^n = a^2 ±na^n-1 +
...
where the remaining terms of higher power in
and therefore negligible. The relative error in z is
zz = na^n-1 a^n =
n a,
while the relative error in a was
. For
example, let
be the measured diameter of
a disk, for which we want the area A. The relationship
between A and d is
. For an uncertainty
in d,
A = (d ±)^2/4 = (d^2 ±2d+
^2)/4. The true value is
giving an error of
if one neglects the
term quadratic in
(and one typically does). This
makes the relative error of
,
twice the relative error in d.
If the desired result is the product of two variables, we
follow a similar procedure.
Let z (actual) = xy be the desired result, with
and
the measured quantities.
Then introducing the uncertainties
z (measured) = (x + x) (y + y) = xy + x
y + y x + ...
and the relative error is, neglecting the terms quadratic in
the uncertainties,
zz = xx +
yy,or the sum of the relative
errors of the individual measurements.
These results follow in more general form from calculus. Let R = f(x, y, z) be the functional relationship between three measurements and the desired result. If one differentiates R, then dR = fxdx + fydy + fzdz, gives the uncertainty in R, when the uncertainties dx, dy, and dz are known.
For example, consider the density of a solid. The
functional relationship is
= mr^2 l,
where m = mass, r = radius, l = length, are the three
measured quantities and = density. Hence,
m = 1r^2 l;
r = -2mr^3 l;
l = -mpi r^2
l^2,
and so
d = 1r^2 l dm + -2mr^3 l dr
+ -2mr^3 l dl.
To get the relative error divide by
obtaining
d = dmm + 2drr +
dll,
where the negative signs have been dropped to estimate the
worst possible combination of errors. We can then express
the relative error in the density so:
= mm +
2rr + ll,
and if one can assume that the errors are distributed
normally, then we can say that
= ( mm
)^2 + ( 2rr )^2 +
(ll)^2 , or
= ( mm
)^2 + ( 2rr )^2
+ (ll)^2 .
Significant figures
Suppose you have measured the diameter of a circular disc and wish to compute its area. A = d^24 = r^2.
Let the average value of the diameter by
mm; dividing d by 2 to get r we obtain
mm with a relative error
of 0.00012.
Squaring r we find,
.
Are we going to use all these digits? NO! Beyond the
uncertainty in r and , one has no experimental
reason for including them, they are insignificant.
The relative error in
is twice that in r so that the
value of
is uncertain to about 4 in the 5th digit
since
is
, i.e.
. There
is clearly no point in carrying figures beyond the 5th in
further calculation. Here, the first five figures are
called significant figures. Now in computing the
area from
, how many digits of
must
be used?
r^2 = 147.94 ×3.1415926535897....?
which gives
. But the relative
error in A is just
which
implies that
. A is uncertain in the
first decimal place. It makes no sense to include digits
for
beyond the second decimal place since those
numbers will not affect the final result.
A rule of rather general applicability is to use one more digit in constants than is available in your measurements, and to save not more than one more digit in computations than the number of significant figures in the data.
Systematic errors in the laboratory standards of length, time, and mass
For the experiments in this manual these systematic
errors are usually negligible compared to other
uncertainties. An exception sometimes occurs for the
larger masses especially the 100 gram, the 500 gram and 1
kg masses. Some contain drilled holes into which lead shot
and a plug have been added to adjust the mass to within
tolerance (typically
. Occasionally a
plug works loose and the calibration lead shot is lost.
You can check the assigned mass values by weighing them on
the triple beam balances. Report any deviations greater
than 0.4% to the instructor.
Acknowledgments
The line drawings were done by Professor Severn, and were, essentially, mere reproductions of sketches done by Professors Estberg, White, and Warren. The first figure in the DC Circuits experiment comes from Guide to Electronic Measurements and Laboratory Practice, by Stanley Wolf. The figures for the Oscilloscope experiment are reprinted from The Art of Electronics, Cambridge University Press, by Horowitz and Hill (the generic oscilloscope), and Laboratory Experiments in Elementary Physics, Waveland Press, by Richards and Rollefson (the Lissajous figures). This document was prepared using LATEX.